I went through a bout of whacky numbers much like yours that didn't make sense. Through process of Elimination and borrowing a members kits found out both my Ca and Alk salifert kits were bad and mr refractometer was off a few clicks. Long story short after all was said and done I abandoned two part and went CaCo3 with a Masterflex to control effluent.. I will add that the saliferts still had 1+ years to go before expiration. And I now calibrate the refrac at every WC just to be sure.
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